6MWW
LasR LBD:BB0126 complex
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RUH3R |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2016-11-17 |
| Detector | RIGAKU RAXIS IV++ |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 50.892, 63.581, 51.797 |
| Unit cell angles | 90.00, 112.17, 90.00 |
Refinement procedure
| Resolution | 23.780 - 2.760 |
| R-factor | 0.208 |
| Rwork | 0.204 |
| R-free | 0.28100 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.150 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHENIX |
| Refinement software | BUSTER (2.10.3) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 23.800 | 2.860 |
| High resolution limit [Å] | 2.760 | 2.760 |
| Number of reflections | 7739 | |
| <I/σ(I)> | 7.6 | |
| Completeness [%] | 97.2 | |
| Redundancy | 3.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 298 | 0.1 M sodium acetate, 30% PEG400 |
