6M4R

Structure of Human Serum Albumin

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2020-01-12
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.98
Spacegroup name	P 1
Unit cell lengths	55.664, 59.099, 86.812
Unit cell angles	90.10, 90.04, 103.60

Refinement procedure

Resolution	19.760 - 2.490
R-factor	0.2342
Rwork	0.232
R-free	0.27360
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1ao6
Refinement software	PHENIX (1.17_3644)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	19.760	2.590
High resolution limit [Å]	2.490	2.490
Rmerge	0.073	0.686
Number of reflections	36927	4168
<I/σ(I)>	8.3
Completeness [%]	98.0
Redundancy	3.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	PEG