6LPG
human VASH1-SVBP complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-1A |
Synchrotron site | Photon Factory |
Beamline | BL-1A |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-03-10 |
Detector | DECTRIS EIGER2 X 4M |
Wavelength(s) | 1.1 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 71.854, 71.854, 215.811 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 47.060 - 2.300 |
R-factor | 0.1942 |
Rwork | 0.190 |
R-free | 0.23620 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6nvq |
RMSD bond length | 0.007 |
RMSD bond angle | 0.851 |
Data reduction software | XDS |
Data scaling software | pointless |
Phasing software | PHASER |
Refinement software | PHENIX (1.17_3644) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.060 | 2.382 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.016 | 0.243 |
Rmeas | 0.023 | 0.344 |
Rpim | 0.016 | 0.243 |
Number of reflections | 15488 | 1492 |
<I/σ(I)> | 24.05 | 2.59 |
Completeness [%] | 99.9 | |
Redundancy | 2 | |
CC(1/2) | 1.000 | 0.860 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.16 M ammonium sulfate, 0.08 M Sodium acetate pH4.6, 20%(w/v) PEG4000, 20%(v/v) glycerol |