6LHM

Structure of human PYCR2

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	AUSTRALIAN SYNCHROTRON BEAMLINE MX1
Synchrotron site	Australian Synchrotron
Beamline	MX1
Temperature [K]	100
Detector technology	CCD
Collection date	2016-10-19
Detector	ADSC QUANTUM 210r
Wavelength(s)	0.97920
Spacegroup name	P 21 2 21
Unit cell lengths	101.903, 110.312, 155.465
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	46.904 - 3.400
R-factor	0.3317
Rwork	0.329
R-free	0.36010
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	2izz
Data reduction software	XDS
Data scaling software	pointless
Phasing software	PHENIX
Refinement software	PHENIX (1.14_3260)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	46.904	3.522
High resolution limit [Å]	3.400	3.400
Number of reflections	24754	20319
<I/σ(I)>	8.75
Completeness [%]	97.7
Redundancy	8.2
CC(1/2)	0.829	0.659

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	0.1M Carboxylic acids, 0.1M Buffer system 3 pH 8.5, 50% v/v Precipitant Mix 3