6KVL

Crystal structure of UDP-RebB-SrUGT76G1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-09-28
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.9798
Spacegroup name	P 31 2 1
Unit cell lengths	97.463, 97.463, 89.899
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	39.674 - 1.998
R-factor	0.1695
Rwork	0.168
R-free	0.20450
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	2vce
RMSD bond length	0.010
RMSD bond angle	1.403
Data reduction software	HKL-3000
Data scaling software	HKL-3000
Phasing software	PHENIX
Refinement software	PHENIX (1.10_2155)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	39.674	2.070
High resolution limit [Å]	1.998	1.998
Rmeas	0.153
Number of reflections	53258	3321
<I/σ(I)>	26.6
Completeness [%]	100.0
Redundancy	11
CC(1/2)	0.994	0.941

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	18% (vol/vol) 2-propanol, 0.1M sodium citrate tribasic dihydrate, pH 5.5, 18% (wt/vol) PEG4000