6JZN

Structure of the intermembrane space region of PARC6-PDV1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U1
Synchrotron site	SSRF
Beamline	BL17U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-06-07
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.979
Spacegroup name	C 2 2 21
Unit cell lengths	91.454, 95.827, 196.566
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	49.142 - 2.894
R-factor	0.2251
Rwork	0.223
R-free	0.27150
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	6jzf
RMSD bond length	0.007
RMSD bond angle	1.260
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX ((1.13_2998: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	49.142	2.997
High resolution limit [Å]	2.890	2.894
Number of reflections	18678	1302
<I/σ(I)>	11.28
Completeness [%]	95.0
Redundancy	7.1
CC(1/2)	0.997	0.904

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		291	sodium acetate, phosphate potassium