6JJ5

BRD4 in complex with 259

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U1
Synchrotron site	SSRF
Beamline	BL17U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-11-26
Detector	DECTRIS PILATUS3 S 6M
Wavelength(s)	0.9793
Spacegroup name	P 21 21 21
Unit cell lengths	32.060, 47.200, 79.120
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	40.535 - 1.200
R-factor	0.1773
Rwork	0.176
R-free	0.20260
Data reduction software	TRUNCATE
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX (1.14_3235)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	40.535	1.243
High resolution limit [Å]	1.200	1.200
Number of reflections	38139
<I/σ(I)>	8.71
Completeness [%]	99.4
Redundancy	2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		295	4.0M HCOONa