6IGE
Crystal structure of Human Papillomavirus type 33 pentamer
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL17U1 |
| Synchrotron site | SSRF |
| Beamline | BL17U1 |
| Temperature [K] | 80 |
| Detector technology | CCD |
| Collection date | 2013-10-20 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.9795 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 98.827, 171.937, 145.692 |
| Unit cell angles | 90.00, 97.04, 90.00 |
Refinement procedure
| Resolution | 48.198 - 2.900 |
| R-factor | 0.2111 |
| Rwork | 0.210 |
| R-free | 0.24030 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 5y9e |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.648 |
| Data scaling software | HKL-2000 |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.970 |
| High resolution limit [Å] | 2.900 | 2.920 |
| Number of reflections | 105277 | 5220 |
| <I/σ(I)> | 14.2 | |
| Completeness [%] | 99.8 | |
| Redundancy | 3.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293.15 | 0.2 M magnesium formate, 13.5% (w/v) PEG 3350 |
