6HY9
THE GLIC PENTAMERIC LIGAND-GATED ION CHANNEL MUTANT Q193M
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 193 |
Detector technology | CCD |
Collection date | 2015-10-04 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9789 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 181.990, 134.360, 159.180 |
Unit cell angles | 90.00, 101.47, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.950 |
R-factor | 0.204 |
Rwork | 0.203 |
R-free | 0.22650 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.100 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | BUSTER |
Refinement software | BUSTER (2.10.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.400 | 3.010 |
High resolution limit [Å] | 2.950 | 2.950 |
Rmerge | 0.064 | |
Number of reflections | 76643 | |
<I/σ(I)> | 11.7 | |
Completeness [%] | 97.0 | 95.6 |
Redundancy | 4 | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 4 | 291 | PH 4, VAPOR DIFFUSION, TEMPERATURE 291K. 12-14.5% PEG4K; 15% GLycerol; 400 mM NaSCN; 3% DMSO; 100mM NaAcetate pH 4. |