Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX1 |
| Synchrotron site | Australian Synchrotron |
| Beamline | MX1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2012-12-18 |
| Detector | ADSC QUANTUM 210r |
| Wavelength(s) | 0.9 |
| Spacegroup name | P 31 2 1 |
| Unit cell lengths | 126.242, 126.242, 296.877 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 19.966 - 1.950 |
| R-factor | 0.1635 |
| Rwork | 0.163 |
| R-free | 0.19900 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4dhl |
| RMSD bond length | 0.007 |
| RMSD bond angle | 0.887 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 19.970 | 2.060 |
| High resolution limit [Å] | 1.950 | 1.950 |
| Rmerge | 0.214 | 1.193 |
| Rmeas | 0.226 | 1.265 |
| Rpim | 0.070 | 0.419 |
| Number of reflections | 199405 | 28831 |
| <I/σ(I)> | 10.6 | 1.9 |
| Completeness [%] | 99.9 | 100 |
| Redundancy | 10.4 | 9 |
| CC(1/2) | 0.994 | 0.585 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5 | 291 | 2.3 M ammonium sulfate, 0.1 M sodium acetate, pH 4.0 |
