6HV1
The apo structure of Dps from Listeria innocua before soaking experiments with Zn, Co and La
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2014-11-11 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 1 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 84.710, 84.710, 263.610 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.761 - 2.547 |
R-factor | 0.1921 |
Rwork | 0.190 |
R-free | 0.22730 |
RMSD bond length | 0.006 |
RMSD bond angle | 0.796 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.761 | 2.610 |
High resolution limit [Å] | 2.547 | 2.547 |
Number of reflections | 59885 | |
<I/σ(I)> | 9.9 | |
Completeness [%] | 99.9 | |
Redundancy | 4.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 20% PEG3350, pH 7 |