6HUI

The structure of Dps from Listeria innocua soaked with zinc

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALBA BEAMLINE XALOC
Synchrotron site	ALBA
Beamline	XALOC
Temperature [K]	100
Detector technology	PIXEL
Collection date	2013-10-10
Detector	DECTRIS PILATUS3 S 6M
Wavelength(s)	0.979260
Spacegroup name	P 41 21 2
Unit cell lengths	86.330, 86.330, 269.298
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	45.696 - 2.995
R-factor	0.2311
Rwork	0.228
R-free	0.28400
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.002
RMSD bond angle	0.403
Data reduction software	XDS
Data scaling software	XDS
Phasing software	MOLREP
Refinement software	PHENIX ((1.10.1_2155: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	45.696	3.180
High resolution limit [Å]	2.995	2.995
Number of reflections	38906
<I/σ(I)>	14.8
Completeness [%]	99.6
Redundancy	8.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7	293	20% PEG-3350, 100 mM Hepes