6HQ9
Crystal structure of the Tudor domain of human ERCC6-L2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-07-08 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.976 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 23.539, 54.399, 108.825 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 54.410 - 1.982 |
R-factor | 0.2255 |
Rwork | 0.224 |
R-free | 0.24730 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3fdr |
RMSD bond length | 0.003 |
RMSD bond angle | 0.524 |
Data reduction software | DIALS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 54.410 | 2.030 |
High resolution limit [Å] | 1.980 | 1.980 |
Rmerge | 0.193 | 4.040 |
Rpim | 0.035 | 0.710 |
Number of reflections | 10359 | 719 |
<I/σ(I)> | 12.8 | 2.1 |
Completeness [%] | 100.0 | 100 |
Redundancy | 31.5 | 32.8 |
CC(1/2) | 0.999 | 0.936 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 0.2 M Ammonium sulphate, 0.1 M Acetate pH 4.5, 18% PEG 4000 |