6HP3

ARBITRIUM PEPTIDE RECEPTOR FROM SPBETA PHAGE

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALBA BEAMLINE XALOC
Synchrotron site	ALBA
Beamline	XALOC
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-12-12
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.97925
Spacegroup name	P 1 21 1
Unit cell lengths	78.907, 251.202, 95.077
Unit cell angles	90.00, 90.89, 90.00

Refinement procedure

Resolution	125.600 - 2.700
R-factor	0.22019
Rwork	0.219
R-free	0.24970
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.018
RMSD bond angle	2.168
Data reduction software	XDS
Data scaling software	SCALA
Phasing software	MOLREP
Refinement software	REFMAC (5.8.0158)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	251.200	2.850
High resolution limit [Å]	2.700	2.700
Number of reflections	101076
<I/σ(I)>	8.1
Completeness [%]	100.0
Redundancy	7.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		294	PEG 3500, sodium chloride, hepes