6HGC
Structure of Calypso in complex with DEUBAD of ASX
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID30B |
Synchrotron site | ESRF |
Beamline | ID30B |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-09-01 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.9747 |
Spacegroup name | P 61 2 2 |
Unit cell lengths | 119.505, 119.505, 408.900 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 72.729 - 3.020 |
R-factor | 0.2695 |
Rwork | 0.268 |
R-free | 0.29170 |
RMSD bond length | 0.003 |
RMSD bond angle | 0.565 |
Refinement software | PHENIX (1.12_2829) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 103.490 | 3.120 |
High resolution limit [Å] | 3.020 | 3.020 |
Number of reflections | 31261 | |
<I/σ(I)> | 13.3 | |
Completeness [%] | 89.3 | |
Redundancy | 18.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293 | 6% PEG MME 5K, 0.1 M HEPES pH 7.0, 5 % Tacsimate |