6H09
HIV capsid hexamer with IP6 ligand
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I02 |
| Synchrotron site | Diamond |
| Beamline | I02 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2017-03-03 |
| Detector | OXFORD RUBY CCD |
| Wavelength(s) | 0.987 |
| Spacegroup name | P 6 |
| Unit cell lengths | 91.099, 91.099, 57.111 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 46.300 - 2.000 |
| R-factor | 0.23914 |
| Rwork | 0.238 |
| R-free | 0.26620 |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.551 |
| Data reduction software | iMOSFLM |
| Data scaling software | pointless |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0230) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 78.900 | 2.110 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Rmeas | 0.898 | |
| Number of reflections | 18396 | |
| <I/σ(I)> | 2 | 2.4 |
| Completeness [%] | 99.7 | 96.5 |
| Redundancy | 4.9 | 4.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | BATCH MODE | 293 | PEG 4K |
