6GW6
Structure of the Pseudomonas putida RES-Xre toxin-antitoxin complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-05-06 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9763 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 60.060, 90.330, 186.640 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 45.165 - 2.205 |
R-factor | 0.2159 |
Rwork | 0.214 |
R-free | 0.25290 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.165 | 2.284 |
High resolution limit [Å] | 2.200 | 2.205 |
Number of reflections | 51891 | |
<I/σ(I)> | 12.25 | |
Completeness [%] | 99.2 | |
Redundancy | 13.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293.15 | 0.2 M Sodium malonate pH 6.0 and 20% w/v Polyethylene glycol 3350 |