6G8W
Crystal Structures of the Single PDZ Domains from GRASP65 and their Interaction with the Golgin GM130
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | BESSY BEAMLINE 14.1 |
Synchrotron site | BESSY |
Beamline | 14.1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2011-05-25 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.91841 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 50.825, 82.613, 49.220 |
Unit cell angles | 90.00, 110.82, 90.00 |
Refinement procedure
Resolution | 26.850 - 2.120 |
R-factor | 0.18839 |
Rwork | 0.186 |
R-free | 0.23548 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3rle |
RMSD bond length | 0.020 |
RMSD bond angle | 1.979 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0189) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 26.850 | 2.180 |
High resolution limit [Å] | 2.120 | 2.120 |
Rmeas | 0.078 | 0.626 |
Number of reflections | 10762 | 788 |
<I/σ(I)> | 15.78 | 2.97 |
Completeness [%] | 99.3 | 100 |
Redundancy | 4.1 | 4.1 |
CC(1/2) | 0.999 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293.15 | 1.4M Na/K phosphate pH 8.2 |