6G1L

MITF/CLEARbox structure

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE MASSIF-1
Synchrotron site	ESRF
Beamline	MASSIF-1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2015-12-05
Detector	DECTRIS PILATUS3 2M
Wavelength(s)	0.966
Spacegroup name	I 21 21 21
Unit cell lengths	44.091, 103.858, 112.894
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	40.585 - 2.400
R-factor	0.2164
Rwork	0.215
R-free	0.25290
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	4ati
RMSD bond length	0.008
RMSD bond angle	0.856
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX ((1.13_2998: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	41.070	2.490
High resolution limit [Å]	2.400	2.400
Rmerge	0.059	0.763
Number of reflections	10459	1087
<I/σ(I)>	12.1	1.7
Completeness [%]	99.5	100
Redundancy	4.4	4.2
CC(1/2)	0.999	0.604

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		294	0.9 M Sodium malonate