6G1L
MITF/CLEARbox structure
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE MASSIF-1 |
Synchrotron site | ESRF |
Beamline | MASSIF-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-12-05 |
Detector | DECTRIS PILATUS3 2M |
Wavelength(s) | 0.966 |
Spacegroup name | I 21 21 21 |
Unit cell lengths | 44.091, 103.858, 112.894 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.585 - 2.400 |
R-factor | 0.2164 |
Rwork | 0.215 |
R-free | 0.25290 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4ati |
RMSD bond length | 0.008 |
RMSD bond angle | 0.856 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.070 | 2.490 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.059 | 0.763 |
Number of reflections | 10459 | 1087 |
<I/σ(I)> | 12.1 | 1.7 |
Completeness [%] | 99.5 | 100 |
Redundancy | 4.4 | 4.2 |
CC(1/2) | 0.999 | 0.604 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 294 | 0.9 M Sodium malonate |