6FZU
RORGT (264-518;C455S) IN COMPLEX WITH THE FRAGMENT ("CPD-1") AND RIP140 PEPTIDE AT 1.80A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X10SA |
Synchrotron site | SLS |
Beamline | X10SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-05-04 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 1.00000 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 47.918, 67.874, 82.451 |
Unit cell angles | 90.00, 101.85, 90.00 |
Refinement procedure
Resolution | 19.800 - 1.800 |
R-factor | 0.2166 |
Rwork | 0.215 |
R-free | 0.25120 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5nti |
RMSD bond length | 0.009 |
RMSD bond angle | 1.068 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.800 | 1.850 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.060 | 0.559 |
Rmeas | 0.072 | 0.699 |
Number of reflections | 46451 | |
<I/σ(I)> | 11.8 | 2.2 |
Completeness [%] | 96.9 | 93.1 |
Redundancy | 3.1 | 2.6 |
CC(1/2) | 0.997 | 0.652 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 298 | 22% PEG3350, 0.2M ammonium acetate, 0.1M bis-TRIS |