Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06DA |
| Synchrotron site | SLS |
| Beamline | X06DA |
| Temperature [K] | 80 |
| Detector technology | PIXEL |
| Collection date | 2014-04-11 |
| Detector | DECTRIS PILATUS 2M-F |
| Wavelength(s) | 1 |
| Spacegroup name | P 31 2 1 |
| Unit cell lengths | 97.810, 97.810, 233.770 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 19.910 - 3.000 |
| R-factor | 0.2669 |
| Rwork | 0.265 |
| R-free | 0.30480 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1tr2 |
| RMSD bond length | 0.002 |
| RMSD bond angle | 0.558 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 19.910 | 19.910 |
| High resolution limit [Å] | 3.000 | 3.000 |
| Number of reflections | 26203 | |
| <I/σ(I)> | 24.68 | |
| Completeness [%] | 97.9 | |
| Redundancy | 19.85 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 277.15 | PEG 4000, calcium acetate, Tris-HOAc, 15% ethylene glycol |
