6FTZ
COMPLEMENT FACTOR D COMPLEXED WITH COMPOUND 6
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2007-10-12 |
| Detector | MARRESEARCH |
| Wavelength(s) | 1.54 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 55.220, 49.975, 39.370 |
| Unit cell angles | 90.00, 106.07, 90.00 |
Refinement procedure
| Resolution | 18.700 - 1.670 |
| R-factor | 0.175 |
| Rwork | 0.173 |
| R-free | 0.22000 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 5fbe |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.090 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | BUSTER (2.11.7) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 49.980 | 1.740 |
| High resolution limit [Å] | 1.670 | 1.670 |
| Rmerge | 0.055 | 0.197 |
| Number of reflections | 23397 | |
| <I/σ(I)> | 10.62 | 5.53 |
| Completeness [%] | 97.1 | 90.6 |
| Redundancy | 3.09 | 2.91 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 295 | PEG3350, 100 mM HEPES pH 7.5 |
