6FOK

Copper transporter OprC

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I02
Synchrotron site	Diamond
Beamline	I02
Temperature [K]	100
Detector technology	PIXEL
Collection date	2015-10-08
Detector	DECTRIS PILATUS 6M-F
Wavelength(s)	1.3785
Spacegroup name	C 2 2 21
Unit cell lengths	156.370, 196.720, 166.350
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	84.670 - 1.970
R-factor	0.211
Rwork	0.210
R-free	0.23200
Structure solution method	SAD
RMSD bond length	0.007
RMSD bond angle	0.925
Data reduction software	xia2
Data scaling software	Aimless
Phasing software	PHENIX
Refinement software	PHENIX ((1.12_2829: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	84.670	2.020
High resolution limit [Å]	1.970	1.970
Number of reflections	178934	0
<I/σ(I)>	15.8
Completeness [%]	99.5
Redundancy	25.4
CC(1/2)	0.990	0.500

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6.5	293	0.1 M NaCl 0.15 M NH4SO4 0.1 M MES 18-22% PEG1000 3 mM CuCl2