6FLC
2C8 Fab bound to EDIII of DenV 2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-2 |
Synchrotron site | ESRF |
Beamline | ID14-2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-07-20 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.98 |
Spacegroup name | P 1 |
Unit cell lengths | 42.560, 61.416, 104.594 |
Unit cell angles | 77.54, 81.11, 85.53 |
Refinement procedure
Resolution | 33.700 - 2.000 |
R-factor | 0.1817 |
Rwork | 0.180 |
R-free | 0.21600 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.130 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | MOLREP |
Refinement software | BUSTER (2.9.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 33.700 | 2.100 |
High resolution limit [Å] | 2.000 | 2.000 |
Number of reflections | 66849 | |
<I/σ(I)> | 15 | |
Completeness [%] | 97.0 | |
Redundancy | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 294 | Read the paper |