6FJF
Tubulin-FcMaytansine complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-11-25 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 1.00036 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 104.373, 156.739, 180.956 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.547 - 2.402 |
R-factor | 0.2033 |
Rwork | 0.201 |
R-free | 0.25750 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 4i4t |
RMSD bond length | 0.002 |
RMSD bond angle | 0.545 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX ((dev_2863: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.600 | 2.460 |
High resolution limit [Å] | 2.400 | 2.400 |
Rmerge | 0.216 | 2.586 |
Rmeas | 0.234 | 2.814 |
Number of reflections | 116072 | 8494 |
<I/σ(I)> | 9.96 | 0.75 |
Completeness [%] | 100.0 | 99.8 |
Redundancy | 6.8 | 6.5 |
CC(1/2) | 0.994 | 0.277 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6.7 | 294 | 10 % PEG 4k, 16 % glycerol, 30 mM MgCl2, 30 mM CaCl2, and 100 mM 2-(N-morpholino)ethanesulfonic acid/imidazole |