6EZY
ARABIDOPSIS THALIANA GSTF9, GSH AND GSOH BOUND
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-08-29 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.9795 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 114.125, 114.125, 89.810 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 49.418 - 2.350 |
R-factor | 0.1583 |
Rwork | 0.156 |
R-free | 0.19660 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4ri6 |
RMSD bond length | 0.012 |
RMSD bond angle | 1.267 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.418 | 2.480 |
High resolution limit [Å] | 2.340 | 2.340 |
Rmerge | 0.112 | |
Number of reflections | 28880 | |
<I/σ(I)> | 18.3 | 1.64 |
Completeness [%] | 98.7 | 96.8 |
Redundancy | 9.9 | 9.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 273 | 0.10M KBr, 30% PEGMME 2000 |