6EW6
Crystal structure of the BCL6 BTB domain in complex with anilinopyrimidine ligand
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 17-ID |
| Synchrotron site | APS |
| Beamline | 17-ID |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2013-06-03 |
| Detector | DECTRIS PILATUS3 S 6M |
| Wavelength(s) | 0.9 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 30.540, 73.010, 53.540 |
| Unit cell angles | 90.00, 104.23, 90.00 |
Refinement procedure
| Resolution | 14.930 - 1.390 |
| R-factor | 0.191 |
| Rwork | 0.190 |
| R-free | 0.22200 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.050 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | BUSTER (2.11.6) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 36.510 | 1.470 |
| High resolution limit [Å] | 1.390 | 1.390 |
| Number of reflections | 22114 | |
| <I/σ(I)> | 19.1 | 3.2 |
| Completeness [%] | 96.8 | 95.2 |
| Redundancy | 4.1 | 4.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | unknown |
