6EVH

Lipoaminopeptide helioferin A and B from Mycogone rosea

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SEALED TUBE
Source details	BRUKER IMUS MICROFOCUS
Temperature [K]	100
Detector technology	CMOS
Collection date	2017-06-07
Detector	RDI CMOS_8M
Wavelength(s)	1.54178
Spacegroup name	C 1 2 1
Unit cell lengths	34.711, 10.886, 17.150
Unit cell angles	90.00, 93.05, 90.00

Refinement procedure

Resolution	17.300 - 0.900
R-factor	0.0856
Rwork	0.085
R-free	0.09320
Structure solution method	AB INITIO PHASING
Data reduction software	PROTEUM PLUS
Data scaling software	SAINT
Phasing software	SHELXS
Refinement software	SHELXL

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	17.300	1.000
High resolution limit [Å]	0.820	0.900
Number of reflections	11314
<I/σ(I)>	26.2
Completeness [%]	91.5
Redundancy	9.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	EVAPORATION		297	slow evaporation in a closed vial