6ERM
HIV Hexamer with ligand
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I02 |
| Synchrotron site | Diamond |
| Beamline | I02 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2017-01-03 |
| Detector | OXFORD RUBY CCD |
| Wavelength(s) | 1 |
| Spacegroup name | P 6 |
| Unit cell lengths | 91.039, 91.039, 56.534 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 78.000 - 2.000 |
| R-factor | 0.18274 |
| Rwork | 0.180 |
| R-free | 0.23509 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 5hgm |
| RMSD bond length | 0.020 |
| RMSD bond angle | 1.908 |
| Data reduction software | MOSFLM |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 78.000 | 2.030 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Number of reflections | 18217 | |
| <I/σ(I)> | 10.8 | |
| Completeness [%] | 100.0 | |
| Redundancy | 9.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | BATCH MODE | 277 | PEG4K |
