6ELQ
Carbon Monoxide Dehydrogenase IV from Carboxydothermus hydrogenoformans
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | BESSY BEAMLINE 14.1 |
| Synchrotron site | BESSY |
| Beamline | 14.1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2016-06-22 |
| Detector | DECTRIS PILATUS3 S 6M |
| Wavelength(s) | 0.91841 |
| Spacegroup name | P 3 2 1 |
| Unit cell lengths | 209.150, 209.150, 93.410 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 45.626 - 2.520 |
| R-factor | 0.2362 |
| Rwork | 0.235 |
| R-free | 0.27470 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.003 |
| RMSD bond angle | 0.534 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.11.1-2575_1168: ???)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 46.700 |
| High resolution limit [Å] | 2.520 |
| Number of reflections | 79240 |
| <I/σ(I)> | 10.5 |
| Completeness [%] | 100.0 |
| Redundancy | 15.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 291 | 20 % (v/v) Polypropoylene glycol 400, 10 % (v/v) 1-Propanol |
