6EB6
Crystal structure of BAX W139A monomer
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-03-21 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9536 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 63.159, 63.159, 82.265 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 32.870 - 2.023 |
R-factor | 0.1729 |
Rwork | 0.171 |
R-free | 0.20130 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5w61 |
RMSD bond length | 0.007 |
RMSD bond angle | 0.734 |
Data reduction software | XDS |
Data scaling software | Aimless (0.5.32) |
Phasing software | PHASER (2.8.1) |
Refinement software | PHENIX ((1.13_2998)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.550 | 2.095 |
High resolution limit [Å] | 2.023 | 2.023 |
Rmerge | 0.063 | 0.526 |
Number of reflections | 12611 | 1200 |
<I/σ(I)> | 21.15 | |
Completeness [%] | 98.4 | |
Redundancy | 10.1 | |
CC(1/2) | 0.999 | 0.952 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | Sodium formate, TCEP |