6E0X
A131E mutant of cyt P460 of Nitrosomonas sp. AL212
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-06-06 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.979 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 48.152, 80.356, 120.033 |
Unit cell angles | 90.00, 95.85, 90.00 |
Refinement procedure
Resolution | 47.924 - 1.974 |
R-factor | 0.2077 |
Rwork | 0.206 |
R-free | 0.24860 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6amg |
RMSD bond length | 0.008 |
RMSD bond angle | 1.038 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX ((dev_3126)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 119.630 | 2.005 |
High resolution limit [Å] | 1.970 | 1.974 |
Rmerge | 0.053 | 1.110 |
Number of reflections | 62608 | 62608 |
<I/σ(I)> | 32 | |
Completeness [%] | 96.1 | |
Redundancy | 1.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5 | 293 | 0.2 M sodium chloride, 0.1 M sodium acetate, PEG 6000 |