6E0T
C-terminal domain of Fission Yeast OFD1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E+ SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-12-12 |
Detector | RIGAKU SATURN 944+ |
Wavelength(s) | 1.54184 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 81.085, 106.717, 64.649 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.091 - 2.020 |
R-factor | 0.2024 |
Rwork | 0.200 |
R-free | 0.24370 |
Structure solution method | MIR |
RMSD bond length | 0.003 |
RMSD bond angle | 0.916 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 29.091 | 2.070 |
High resolution limit [Å] | 2.020 | 2.030 |
Number of reflections | 18232 | 756 |
<I/σ(I)> | 28 | |
Completeness [%] | 96.9 | 82.4 |
Redundancy | 6.8 | 4.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 291 | 1.2 M LiSo4, 0.1 M HEPES |