6DNM

The crystal structure of SatS c-terminal domain

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 23-ID-D
Synchrotron site	APS
Beamline	23-ID-D
Temperature [K]	120
Detector technology	PIXEL
Collection date	2018-04-14
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.979
Spacegroup name	P 21 21 21
Unit cell lengths	48.867, 50.580, 76.465
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	42.186 - 1.397
R-factor	0.1947
Rwork	0.193
R-free	0.23070
RMSD bond length	0.005
RMSD bond angle	0.736
Data reduction software	HKL-3000
Data scaling software	HKL-3000
Phasing software	PHENIX
Refinement software	PHENIX ((1.11.1_2575: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	99.000	1.420
High resolution limit [Å]	1.400	1.400
Rmerge	0.081	0.254
Number of reflections	35457
<I/σ(I)>	14.4
Completeness [%]	92.6
Redundancy	5.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		289	3.5M ammonium citrate