6DK4

Crystal structure of Campylobacter jejuni peroxide stress regulator

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 17-ID
Synchrotron site	APS
Beamline	17-ID
Temperature [K]	100
Detector technology	PIXEL
Collection date	2013-01-25
Detector	DECTRIS PILATUS 6M
Wavelength(s)	1.2822
Spacegroup name	P 21 21 21
Unit cell lengths	48.110, 70.186, 85.158
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	54.000 - 2.710
R-factor	0.2176
Rwork	0.215
R-free	0.27010
RMSD bond length	0.010
RMSD bond angle	1.210
Data reduction software	XDS
Data scaling software	autoPROC
Phasing software	AutoSol
Refinement software	BUSTER (2.10.1)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	54.000	2.720
High resolution limit [Å]	2.710	2.710
Number of reflections	8254
<I/σ(I)>	24
Completeness [%]	100.0
Redundancy	14.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		277.15	0.1 M HEPES, pH 7.2-7.4, 35-60% MPD