6DFW
TCR 8F10 in complex with IAg7-p8G9E
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 24-ID-C |
| Synchrotron site | APS |
| Beamline | 24-ID-C |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2015-04-11 |
| Detector | DECTRIS PILATUS3 S 6M |
| Wavelength(s) | 0.979500 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 93.094, 102.044, 136.001 |
| Unit cell angles | 90.00, 107.83, 90.00 |
Refinement procedure
| Resolution | 50.010 - 3.200 |
| R-factor | 0.23619 |
| Rwork | 0.233 |
| R-free | 0.29691 |
| RMSD bond length | 0.023 |
| RMSD bond angle | 2.124 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0135) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 3.500 |
| High resolution limit [Å] | 3.200 | 3.200 |
| Number of reflections | 38891 | |
| <I/σ(I)> | 7.6 | |
| Completeness [%] | 96.9 | |
| Redundancy | 3.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 298 | 11% PEG 3350, 100mM formate pH7.0 |
