6CXG
anti-HIV-1 Fab 2G12 in complex with glycopeptide 10V1S
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL12-2 |
Synchrotron site | SSRL |
Beamline | BL12-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2015-08-05 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97950 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 45.221, 131.179, 169.541 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.385 - 2.298 |
R-factor | 0.1992 |
Rwork | 0.197 |
R-free | 0.23720 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4rbp |
RMSD bond length | 0.009 |
RMSD bond angle | 1.349 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.12_2829: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.400 | 2.340 |
High resolution limit [Å] | 2.298 | 2.298 |
Rmerge | 0.174 | 1.000 |
Rmeas | 0.193 | 1.000 |
Rpim | 0.095 | 0.506 |
Number of reflections | 45804 | 2195 |
<I/σ(I)> | 8.8 | 1.9 |
Completeness [%] | 99.5 | 97.6 |
Redundancy | 5.4 | 5.1 |
CC(1/2) | 0.990 | 0.510 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 295 | 1M citrate, 10mM sodium borate |