Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 19-BM |
| Synchrotron site | APS |
| Beamline | 19-BM |
| Temperature [K] | 80 |
| Detector technology | CCD |
| Collection date | 2006-01-01 |
| Detector | APEX II CCD |
| Wavelength(s) | 0.97937 |
| Spacegroup name | P 1 |
| Unit cell lengths | 38.308, 57.767, 65.657 |
| Unit cell angles | 91.32, 89.99, 90.88 |
Refinement procedure
| Resolution | 19.000 - 1.800 |
| R-factor | 0.16364 |
| Rwork | 0.161 |
| R-free | 0.21125 |
| Structure solution method | SAD |
| RMSD bond length | 0.020 |
| RMSD bond angle | 1.965 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | SOLVE |
| Refinement software | REFMAC (5.8.0189) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.860 |
| High resolution limit [Å] | 1.800 | 1.800 |
| Rmerge | 0.077 | 0.144 |
| Number of reflections | 50614 | 49555 |
| <I/σ(I)> | 27.9 | |
| Completeness [%] | 97.6 | 96.9 |
| Redundancy | 4.3 | 4.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 289 | 24% PEG2000 MME, 300 mM sodium chloride, 100 mM HEPES, pH 7.5 |
