6CJL
Candida albicans Hsp90 nucleotide binding domain in complex with radicicol
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | CLSI BEAMLINE 08ID-1 |
| Synchrotron site | CLSI |
| Beamline | 08ID-1 |
| Temperature [K] | 120 |
| Detector technology | CCD |
| Collection date | 2015-08-25 |
| Detector | RAYONIX MX-300 |
| Wavelength(s) | 0.97949 |
| Spacegroup name | P 43 |
| Unit cell lengths | 73.100, 73.100, 109.514 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 37.597 - 1.697 |
| Rwork | 0.145 |
| R-free | 0.16530 |
| Data reduction software | HKL-3000 |
| Data scaling software | HKL-3000 |
| Phasing software | PHASER |
| Refinement software | PHENIX |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.760 |
| High resolution limit [Å] | 1.670 | 1.670 |
| Rmerge | 0.100 | 0.500 |
| Number of reflections | 66682 | 9675 |
| <I/σ(I)> | 14.6 | 4.7 |
| Completeness [%] | 99.9 | 99.8 |
| Redundancy | 9.9 | 9.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5 | 298.15 | 8% Tacsimate 20% PEG3350 |
