6CJL

Candida albicans Hsp90 nucleotide binding domain in complex with radicicol

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	CLSI BEAMLINE 08ID-1
Synchrotron site	CLSI
Beamline	08ID-1
Temperature [K]	120
Detector technology	CCD
Collection date	2015-08-25
Detector	RAYONIX MX-300
Wavelength(s)	0.97949
Spacegroup name	P 43
Unit cell lengths	73.100, 73.100, 109.514
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	37.597 - 1.697
Rwork	0.145
R-free	0.16530
Data reduction software	HKL-3000
Data scaling software	HKL-3000
Phasing software	PHASER
Refinement software	PHENIX

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	1.760
High resolution limit [Å]	1.670	1.670
Rmerge	0.100	0.500
Number of reflections	66682	9675
<I/σ(I)>	14.6	4.7
Completeness [%]	99.9	99.8
Redundancy	9.9	9.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	5	298.15	8% Tacsimate 20% PEG3350