6CFF
Stimulator of Interferon Genes Human
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL12-2 |
Synchrotron site | SSRL |
Beamline | BL12-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-11-25 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97946 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 110.930, 110.930, 36.030 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.090 - 2.396 |
R-factor | 0.19833 |
Rwork | 0.193 |
R-free | 0.24918 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.013 |
RMSD bond angle | 1.701 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 2.457 |
High resolution limit [Å] | 2.396 | 2.396 |
Rmerge | 0.089 | 0.810 |
Rmeas | 0.100 | |
Rpim | 0.048 | 0.330 |
Number of reflections | 8466 | |
<I/σ(I)> | 9.5 | 2.4 |
Completeness [%] | 97.9 | 99.3 |
Redundancy | 4.3 | 4.5 |
CC(1/2) | 0.794 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.2 | 285 | Sodium citrate tribasic, PEG 3350, pH 8.2 |