6C5D

N-terminal domain of Helicobacter pylori LlaJI.R1

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 24-ID-C
Synchrotron site	APS
Beamline	24-ID-C
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-04-21
Detector	DECTRIS PILATUS 6M-F
Wavelength(s)	0.9791
Spacegroup name	P 1
Unit cell lengths	37.526, 43.771, 85.091
Unit cell angles	97.87, 93.86, 97.77

Refinement procedure

Resolution	83.970 - 1.970
Structure solution method	MOLECULAR REPLACEMENT
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	83.970	2.100
High resolution limit [Å]	1.970	1.970
Rmeas	0.096	0.624
Number of reflections	152937	23180
<I/σ(I)>	9	1.56
Completeness [%]	93.6	90.1
Redundancy	3.68	1.91
CC(1/2)	0.997	0.709

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	6.5	298	0.1 M MMT, pH 6.5, 25% v/v PEG1500