6C10

Crystal structure of mouse PCDH15 EC11-EL

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 24-ID-C
Synchrotron site	APS
Beamline	24-ID-C
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-06-18
Detector	DECTRIS PILATUS 6M-F
Wavelength(s)	0.98
Spacegroup name	P 43 21 2
Unit cell lengths	57.680, 57.680, 159.180
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	54.230 - 1.399
R-factor	0.1706
Rwork	0.169
R-free	0.19510
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.006
RMSD bond angle	0.733
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	Auto-Rickshaw
Refinement software	PHENIX ((1.12_2829: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	54.230	1.450
High resolution limit [Å]	1.400	1.400
Number of reflections	53914
<I/σ(I)>	25.05
Completeness [%]	99.7
Redundancy	9.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	8.5	293	0.2 M Lithium sulfate, 30% (w/v) PEG4000, 0.1 M Tris pH 8.5