6BXV
SYSSYGQS from low-complexity domain of FUS, residues 54-61
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2014-08-13 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9791 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 49.580, 4.785, 21.812 |
Unit cell angles | 90.00, 95.46, 90.00 |
Refinement procedure
Resolution | 24.680 - 1.100 |
R-factor | 0.1378 |
Rwork | 0.137 |
R-free | 0.14770 |
Structure solution method | AB INITIO PHASING |
RMSD bond length | 0.004 |
RMSD bond angle | 0.755 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | SHELXD |
Refinement software | REFMAC (5.8.0073) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 100.000 | 100.000 | 1.140 |
High resolution limit [Å] | 1.100 | 2.370 | 1.100 |
Rmerge | 0.139 | 0.073 | 0.514 |
Rmeas | 0.147 | 0.077 | 0.583 |
Rpim | 0.046 | 0.024 | 0.268 |
Total number of observations | 18606 | ||
Number of reflections | 2168 | 232 | 196 |
<I/σ(I)> | 6.9 | ||
Completeness [%] | 90.9 | 86.9 | 82 |
Redundancy | 8.6 | 8.1 | 4.2 |
CC(1/2) | 0.991 | 0.732 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 298 | 0.5M ammonium tartrate dibasic pH 7.0 |