6BP6

Crystal structure of Commd9 COMM domain

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	AUSTRALIAN SYNCHROTRON BEAMLINE MX2
Synchrotron site	Australian Synchrotron
Beamline	MX2
Temperature [K]	100
Detector technology	CCD
Collection date	2017-03-15
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.9787
Spacegroup name	I 4
Unit cell lengths	79.404, 79.404, 58.572
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	30.366 - 2.170
R-factor	0.2514
Rwork	0.248
R-free	0.28550
Structure solution method	SAD
RMSD bond length	0.004
RMSD bond angle	0.637
Data reduction software	MOSFLM
Data scaling software	Aimless
Phasing software	AutoSol
Refinement software	PHENIX ((1.13rc1_2954: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	47.130	2.240
High resolution limit [Å]	2.170	2.170
Rmerge	0.060
Number of reflections	9689
<I/σ(I)>	26.7
Completeness [%]	99.7
Redundancy	13.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	8	293	0.1 M HEPES (pH 7.0), 6% Jeffamine M-600