6BN1
Salvador Hippo SARAH domain complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL12-2 |
Synchrotron site | SSRL |
Beamline | BL12-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-05-28 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97946 |
Spacegroup name | P 43 2 2 |
Unit cell lengths | 49.934, 49.934, 186.169 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.903 - 2.600 |
R-factor | 0.2042 |
Rwork | 0.202 |
R-free | 0.24590 |
RMSD bond length | 0.007 |
RMSD bond angle | 0.952 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.903 | 2.900 |
High resolution limit [Å] | 2.600 | 2.600 |
Number of reflections | 7868 | |
<I/σ(I)> | 10.6 | |
Completeness [%] | 100.0 | |
Redundancy | 24.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 298 | 100 mM Sodium Cacadylate 35% MPD 2% PEG 20K |