6BME
Crystal structure of Chlamydomonas reinhardtii THB4
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SEALED TUBE |
Source details | OTHER |
Temperature [K] | 110 |
Detector technology | CCD |
Collection date | 2017-06-27 |
Detector | AGILENT ATLAS CCD |
Wavelength(s) | 1.54 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 74.400, 68.300, 49.400 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.677 - 1.899 |
R-factor | 0.1915 |
Rwork | 0.188 |
R-free | 0.22690 |
Structure solution method | SAD |
RMSD bond length | 0.008 |
RMSD bond angle | 0.736 |
Data reduction software | CrysalisPro (1.171.36.32) |
Data scaling software | CrysalisPro (1.171.36.32) |
Phasing software | PHENIX (1.11.1_2575) |
Refinement software | PHENIX (1.11.1_2575: ???) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.680 | 1.970 |
High resolution limit [Å] | 1.899 | 1.899 |
Rmerge | 0.028 | 0.169 |
Number of reflections | 38306 | 3832 |
<I/σ(I)> | 32.37 | 5 |
Completeness [%] | 99.9 | 100 |
Redundancy | 8.5 | 6.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 295 | 0.2 M Ammonium Sulfate, 0.1 M Bis-Tris pH 5.5, 20% PEG 3350 |