6B7L
Aeromonas veronii immune modulator A
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.2 |
Synchrotron site | ALS |
Beamline | 5.0.2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-07-16 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 1.0 |
Spacegroup name | P 6 2 2 |
Unit cell lengths | 160.465, 160.465, 66.180 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 41.142 - 2.300 |
R-factor | 0.1756 |
Rwork | 0.172 |
R-free | 0.20400 |
Structure solution method | SAD |
RMSD bond length | 0.008 |
RMSD bond angle | 1.099 |
Data scaling software | SCALA |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.246 | 2.300 |
High resolution limit [Å] | 2.300 | 2.300 |
Number of reflections | 22818 | 3244 |
<I/σ(I)> | 16.1 | 1.4 |
Completeness [%] | 100.0 | 100 |
Redundancy | 70.2 | 71.6 |
CC(1/2) | 1.000 | 0.900 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 294 | 3.5 M sodium formate 15% PEG 200 75 mM NaCl, 25 mM HEPES pH 7.9, 2.5 mM BME |