6B6J
Structure of profilin Art v4
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2017-04-07 |
Detector | RAYONIX MX300-HS |
Wavelength(s) | 1.0 |
Spacegroup name | P 31 |
Unit cell lengths | 32.675, 32.675, 81.782 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 28.300 - 1.900 |
R-factor | 0.16976 |
Rwork | 0.167 |
R-free | 0.21411 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5em0 |
RMSD bond length | 0.014 |
RMSD bond angle | 1.703 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 1.930 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.055 | 0.327 |
Rmeas | 0.065 | 0.368 |
Rpim | 0.040 | 0.233 |
Number of reflections | 7348 | 374 |
<I/σ(I)> | 27.99 | 3.52 |
Completeness [%] | 95.5 | 97.7 |
Redundancy | 2.3 | 2.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.9 | 298 | 0.49 M Sodium phosphate monobasic monohydrate |