6B3I
Annexin A13a
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 21-ID-G |
| Synchrotron site | APS |
| Beamline | 21-ID-G |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2014-06-12 |
| Detector | MARRESEARCH |
| Wavelength(s) | 0.9786 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 190.623, 93.815, 94.858 |
| Unit cell angles | 90.00, 106.02, 90.00 |
Refinement procedure
| Resolution | 39.909 - 2.600 |
| R-factor | 0.1946 |
| Rwork | 0.193 |
| R-free | 0.22960 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1w3w |
| RMSD bond length | 0.002 |
| RMSD bond angle | 0.348 |
| Data reduction software | HKL-2000 |
| Data scaling software | HKL-2000 |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 2.600 |
| Number of reflections | 49419 |
| <I/σ(I)> | 11.7 |
| Completeness [%] | 98.9 |
| Redundancy | 2.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 100 mM NaAcetate, 40 mM 1,2-butanediol, 0.8% PEG 8000 |
