6AYH
Salmonella enterica GusR
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-10-08 |
Detector | MARMOSAIC 300 mm CCD |
Wavelength(s) | 0.97939 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 52.686, 55.230, 60.499 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 27.615 - 2.050 |
R-factor | 0.1871 |
Rwork | 0.183 |
R-free | 0.22200 |
Structure solution method | SAD |
RMSD bond length | 0.003 |
RMSD bond angle | 0.509 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.12_2829) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 27.620 |
High resolution limit [Å] | 2.050 |
Number of reflections | 20844 |
<I/σ(I)> | 10.3 |
Completeness [%] | 99.1 |
Redundancy | 5.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 298.15 | 25% PEG3350, 0.2M Ammonium Acetate, 0.1M Bis-Tris pH6.5 |